homogeneity of variance — 中文翻译 - homogeneity中文
Follow the preceding instructions to troubleshoot and resolve needle bending issues in your GC system. If the problem persists contact Agilent customer support for expert assistance.
If the application requires a cool on-column inlet, make sure that you are using the on-column needle guide (Figure 1). The on-column needle guide provides enhanced support and improved needle guidance. The on-column needle guide can be effectively used also with other inlets when a 5 μL syringe is used.
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If the needle feels loose during operation, adjust the flange guide and the green part holding the syringe latch (Figure 2). Proper adjustment prevents needle movement, minimizing the risk of bending during injections.
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To maintain the elasticity of the rubber septa, avoid over-tightening the septum nut. Excessive tightening can lead to the rubber septa losing its flexibility, causing it to become rigid and hindering the needle's ability to pierce through effectively.For inlet pressures up to 100 psi, tighten the septum retainer until the C-ring lifts about 1 mm above the top surface (Figure 3).
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If application permits, switch from a low volume syringes to a 10 μL syringes. A 10 μL syringe with a thicker needle provides better durability and precision.
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Verify that the needle is correctly installed and has a secure placement (see the article Removing and Installing a Syringe on the Agilent 7693A Autosampler).
Agilent vials and caps should be used. An improper gripping of the vial could occur when using non-Agilent vials or caps with the wrong dimensions, resulting into problems when the needle is going down into the vial.
This procedure is adequate for most situations (See the article Replacing the Inlet Septum for Split/Spitless and Multimode Inlets).
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If the injector is not correctly aligned, the needle could also bend during injection. If you suspect a problem with the alignment, please proceed to align your ALS system. The alignment process may vary depending on the type of injector you have. See the articles How to Align the Agilent 7693A GC Injector and How to Align the Agilent 7683B GC Injector for specific instructions on aligning each type respectively. If your injector differs from the ones listed, contact your local Agilent service representative for assistance.
Translations in context of "Apertur" in German-English from Reverso Context: numerische Apertur.
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